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زمین شیمی فلزات سنگین در پساب‌های ورودی و آب رودخانه کارون محدوده استان خوزستان

تعداد 188صفحه فایل word قابل ویرایش

چکیده

 

زمین شیمی فلزات سنگین در پساب‌های ورودی و آب رودخانه کارون محدوده استان خوزستان

کارون طولانی­ترین و تنها رودخانه قابل کشتیرانی در ایران است. بسیاری از صنایع مانند صنایع فلزی، پتروشیمی و صنایع نفتی در اطراف این رود­خانه قرار دارند. این رود­خانه نیاز آب صنایع حاشیه خود و همچنین آب آشامیدنی شهرهایی مانند اهواز، آبادان و خرمشهر را تأمین می­کند. در این مطالعه 38 نمونه آب و 28 نمونه پساب ورودی به رودخانه کارون جهت بررسی غلظت فلزات سنگینAl, As, Cd Co, Cr, Cu, Fe, Mn, Mo, Ni, Pb) Sb, Se, Zn, V , (Hg جمع­آوری و تجزیه شدند. نتایج نشان داد که نمونه­های آب حوضه آبریز کارون دو تیپ را نشان می­دهند، به طوری که رودخانه دز تیپ بیکربنات تا سولفات و رودخانه کارون تیپ کلروره دارند. نتایج تجزیه شیمیایی نشان داد که غلظت بالای برخی فلزات در نمونه­های آب رودخانه به نواحی مجاور تخلیه پساب واحدهای صنعتی و کشاورزی به رودخانه محدود می­شود. مقایسه غلظت فلزات سنگین در نمونه­های آب رودخانه با میانگین غلظت آنها در رودخانه­های جهان  نشان می­دهد غلظت عناصر سرب، آهن، منگنز، وانادیم، آنتیموان و روی در منطقه مورد مطالعه افزایش یافته است. در این مطالعه مهم­ترین عنصر آلاینده در حوضه آبریز کارون جیوه است. به طور کلی می­توان نتیجه گرفت آلودگی به سمت خلیج فارس، افزایش می یابد.

کلید واژه­ها : آب، پساب ورودی به رودخانه، حوضه آبریز کارون، فلزات سنگین

 

فهرست مطالب

 

عنوان                                                                                                                     صفحه

فصل اول: کليات و مروری بر مطالعات پیشین

1-1- مقدمه. 2

1-2- رودخانه­ها 3

1-3- محیط زمین شیمیایی آب و ارزیابی زیست­محیطی آن.. 3

        1-4- فلزات سنگین…………………………………………………………………….5

     1-4-1- منابع طبیعی ورود عناصر به محیط……………………………………… 6

    1-4-2- منابع انسان­زاد آلودگی فلزات سنگین.. 7

1-5- توزیع فلزات سنگین در محیط آب……………………………………………….8

    1-5-1- آرسنیک… 8

             1-5-2- سرب…………………………………………………………………………………..9

             1-5-3- آلومینیوم……………………………………………………………………………10

             1-5-4-جیوه………………………………………………………………………………….10

             1-5-5-کادمیم……………………………………………………………………………… 11

             1-5-6- روی………………………………………………………………………………….11

             1-5-7-مس ………………………………………………………………………………….12

             1-5-8-نیکل  ………………………………………………………………………………..13

             1-5-9-کبالت ………………………………………………………………………………..13

    1 -5-10- آهن.. 14

   1-5-11- کروم. 14

عنوان                                                                                                                     صفحه

            1-5-12- مولیبدن……………………………………………………………………………15

             1-5-13- منگنز……………………………………………………………………………….15

           1-5-14- سلنیم………………………………………………………………………………..16

      1-6- آنیون و کاتیون­های اصلی در آب………………………………………………………… 17

 1 -6-1- کلسیم.. 17

  1-6-2- منیزیم.. 17

          1-6-3- سدیم……………………………………………………………………………………17

  1-6-4- پتاسیم    18

  1-6-5 – بیکربنات.. 18

   1-6-6-کلر. 18

   1-6-7- سولفات 19

   1-6-8- نیترات و نیتریت… 19

1-7-  مطالعات پیشین ……………………………………………………………… 19

1-8- ضرورت اجرای پژوهش 21

فصل دوم: موقعیت جغرافیایی و جغرافیایی منطقه مورد مطالعه

2-1- مقدمه. 24

2-2- ویژگی­های جغرافیایی استان خوزستان.. 25

    2-2-1- اقلیم.. 25

    2 -2-2- رودخانه ها …………………………………………………………….. 25

               2-2-2-1- رودخانه کارون………………………………………………………………..26

               2-2-2-2- رودخانه دز ………………………………………………………………….. 26

         2-3- ویژگی­های آب و هوایی استان………………………………………………………… 26

          2-4- صنعت……………………………………………………………………………………. 26

     2-4-1- صنعت نفت… 28

عنوان                                                                                                                     صفحه

    2-4-2- صنایع موجود در حاشیه رودخانه کارون.. 28

         2-4-2-1- صابون سازی خرمشهر. 29

         2-4-2-2-نیروگاه رامین  29

          2-4-2-3- کارخانه کاغذ پارس… 30

          2-4-2-4 –پالایشگاه نفت آبادان.. 30

          2-4-2-5- پتروشیمی آبادان.. 31

          2-4-2-6-حوضچه­های پرورش ماهی.. 31

        2-5- کشاورزی در خوزستان…………………………………………………………………..32

    2-5-1-کشت نیشکر در خوزستان.. 34

 2-6- حوضه آبریز کارون …………………………………………………………… 34

            2-6-1- بخش میانی حوضه آبریز کارون…………………………………………………..37

            2-6-2-بخش غربی حوضه آبریز کارون……………………………………………………38

       2-7- زمین شناسی منطقه……………………………………………………………………….38

        2-8- چینه شناسی منطقه مورد مطالعه………………………………………………………..40

          2-8-1- چینه­شناسی نواحی جنوب، غرب و جنوب شرق استان…………………………40

               2-8-1-1- سازند گچساران ……………………………………………………………….41

               2-8-1-2- سازند میشان……………………………………………………………………42

               2-8-1-3- سازند آغاجاری……………………………………………………………….. 42

             2-8-1-4- بخش لهبری …………………………………………………………………. 42

             2-8-1-5- سازند بختیاری…………………………………………………………………44

              2-8-1-6- نهشته های کواترنر……………………………………………………………..44

          2-8-2- چینه­شناسی نواحی شمال، شمال شرق و شمال غرب  ………………………..45

             2-8-2-1- سازند سورمه……………………………………………………………………..45

             2-8-2-2- کژدمی…………………………………………………………………………….46

             2-8-2-3- سروک ……………………………………………………………………………47

عنوان                                                                                                                     صفحه

             2-8-2-4- سورگاه…………………………………………………………………………….47

            2-8-2-5- ایلام……………………………………………………………………………….48

              2-8-2-6- گورپی…………………………………………………………………………….48

            2-8-2-7- پابده……………………………………………………………………………….49

            2-8-2-8- آسماری…………………………………………………………………………..49

فصل سوم: مواد و روش­ها

3-1- مقدمه. 52

3-2- روش نمونه برداری و آماده‌سازی نمونه‌های آب و پساب­های ورودی به  حوضه

                  آبریز کارون…………………………………………………………….57   

 3-3- روش‌های تجزیه‌ای    60

            3-3-1- اساس کار روش ICP-MS ……………………………………………………….60

              3-3-2- اندازه‌گیری کاتیون و آنیون‌های اصلی و نیترات ………………………………61

                 3-3-2-1- تعیین مقدار سدیم نمونه‌های آب  ……………………………………… 61

                  3-3-2-2- تعیین مقدار پتاسیم   …………………………………………………… 61

                3-3-2-3- تعیین مقدار کلسیم …………………………………………………….. 62

                   3-3-2-4- تعیین مقدار منیزیم ……………………………………………………. 62

                 3-3-2-5- تعیین مقدار کلر به روش مور(mohr) ………………………………. 62

                 3-3-2-6- تعیین کربنات و بی‌کربنات ………………………………………………62

                 3-3-2-7- تعیین سولفات نمونه‌های آب …………………………………………..63

 3-4- پارامترهای فیزیکی و شیمیایی مورد بررسی ………………………………. 63

            3-4-1-pH…………………………………………………………………………………… 63

              3-4-2- هدایت الکتریکی(Electrical Conductivity) ………………………………..64

              3-4-3- TDS (Total Dissolved Solid ) ……………………………………………. 64

3-5- تحلیل داده­ها 65

عنوان                                                                                                   صفحه

3-5-1- روش‌های زمین شیمیایی تحلیل داده‌ها  …………………………………….65

            3-5-1-1- ضریب تمایز……………………………………………………………………. 65

              3-5-1-2- سختی کل برحسب کربنات کلسیم (TH) ………………………………….66

              3-5-1-3- نسبت جذب سدیم (Sodium Adsorption Ratio ) …………………….66

            3-5-1-4- درصد سدیم محلول (SSP ) ………………………………………………….67

3-5-2- نمودار­ها 68

            3-5-2-1- نمودار پایپر……………………………………………………………………….68

              3-5-2-2- نمودار ویلکاکس…………………………………………………………………69

3-5-3-روش­های آماری.. 69

   3-5-3-1- آمارتوصیفی ((Descriptive Statistics 70

   3-5-3-2- تحلیل خوشه‌ای 70

   3-5-3- 3- تحلیل مولفه‌های اصلی (PCA) 70

فصل چهارم: فلزات سنگین در آب و پساب­های ورودی به حوضه آبریز کارون 

4-1- بررسی آب و پساب‌های ورودی به حوضه آبریز کارون ……………………….. 73

            4-1-1- پارامترهای فیزیکوشیمیایی……………………………………………………….73

                4-1-1-1- کلسیم ……………………………………………………………………….82

                 4-1-1-2- منیزیم  ………………………………………………………………………84

                   4-1-1-3- پتاسیم……………………………………………………………………….85

                4-1-1-4- سدیم …………………………………………………………………………86

                4-1-1-5- کلر ……………………………………………………………………………88

                4-1-1-6- سولفات……………………………………………………………………….89

                4-1-1-7- بیکربنات …………………………………………………………………….91

                4-1-1-8- نیترات ………………………………………………………………………..92

عنوان                                                                                                                     صفحه

       4-1-2- نمودار پایپر ………………………………………………………………………………97

       4-1-3- نمودار ویلکاکس ………………………………………………………………………100

       4 -1-4- سختی آب …………………………………………………………………………….102

       4-1-5- درصد سدیم محلول (SSP) ………………………………………………………….104

    4-2- فلزات سنگین …………………………………………………………………….105

4-2-1- آلومینیم.. 112

4-2-2- آرسنیک……………………………………………………………………113

         4-2-3- کبالت …………………………………………………………………………………115

          4-2-4- مس ……………………………………………………………………………………116

          4-2-5- آهن ……………………………………………………………………………………118

         4-2-6- منگنز ………………………………………………………………………………….120

         4-2-7- مولیبدن ………………………………………………………………………………121

           4-2-8- نیکل …………………………………………………………………………………123

          4-2-9- سرب …………………………………………………………………………………125

           4-2-10- آنتیموان ……………………………………………………………………………126

          4-2-11- سلنیم ……………………………………………………………………………..127

          4-2-12- روی ………………………………………………………………………………..129

          4-2-13- وانادیم ……………. ………………………………………………………………130

          4-2-14- جیوه ……………………………………………………………………………….132

       4-3- مقایسه میانگین غلظت عناصر آب حوضه آبریز کارون با برخی دیگر از          

                             رودخانه­های جهان…………………………………………………………..133

      4-4-تحلیل داده‌ها  با استفاده از روش‌های زمین شیمیایی …………………………..135

4-4-1- ضریب تمایز ……………………………………………………………….135

           4-4-1-1- نمونه­های آب ………………………………………………………..135

           4-4-1-2- نمونه­های پساب ……………………………………………………..141

عنوان                                                                                               صفحه

              4 -4-1-3- تغییرات غلظت جیوه در نمونه های آب رودخانه و پساب…………145

  4-4-2- تحلیل داده ها  با استفاده از روش های آماری  …………………………146

       4-4-2-1- تجزیه خوشه ای (Cluster Analysis) ……………………………148

       4 -4-2- 2- تحلیل مولفه اصلی (Principal Component Analysis-PCA). 151

               4-4-2-3- مقایسه میانگین غلظت عناصر در آب و پساب (t- test) ……………153

فصل پنجم: نتیجه گیری و پیشنهادات

5-1- نتیجه گیری.. 156

2-5- پیشنهاد برای مطالعات آینده. 159

منابع

منابع فارسی.. 160

منابع انگلیسی.. 163

چکیده و صفحه عنوان به انگلیسی

فهرست جداول

عنوان                                                                                                                     صفحه

جدول 2-1- ‌میزان تولید برخی از محصولات کشاورزی و سهم و رتبه استان  . 33

         جدول 3-1- مختصات جغرافیایی و نام ایستگاه­های نمونه­ برداری از آب

                         رودخانه …………………………………………………………………55

جدول3-2- مختصات جغرافیایی و نام ایستگاه­های نمونه­برداری از پساب­های     

                           ورودی به رودخانه …………………………………………………….56

جدول3-3- رده بندی کیفی آب بر حسب هدایت الکتریکی.. 64

جدول3-4- رده بندی کیفی آب شرب.. 64

         جدول 3-5- تقسیم­بندی آب سطحی جهت کشاورزی  ………………………………65

جدول 3-6- تقسیم بندی آب بر اساس سختی  ……………………………………..66

        جدول3-7- رده بندی آب بر حسب SAR ……………………………………………………67

        جدول 3-8- رده بندی آب بر حسب درصد سدیم …………………………………….68

        جدول 4-1- غلظت یونها و  پارامترهای اصلی  نمونه‌های آب برداشت شده از حوضه

                          آبریز کارون    ………………………………………………………….74

        جدول 4-2- غلظت یونها و  پارامترهای اصلی  نمونه‌های پساب ورودی به حوضه

                            آبریز کارون……………………………………………………………76

         جدول 4-3- خلاصه آماری پارامترهای فیزیکوشیمیایی نمونه های آب رودخانه….   78

جدول 4-4- خلاصه آماری پارامترهای فیزیکوشیمیایی نمونه های پساب ورودی  

                 به آب رودخانه…………………………………………………………..78

 جدول 4-5- نتایج TDS نمونه­های آب و پساب ورودی به رودخانه. 81

جدول 4-6- طبقه بندی آب­های سطحی جهت کشاورزی بر اساس EC و SAR 100

عنوان                                                                                                     صفحه

جدول 4-7- SAR و EC نمونه­های آب و زهکش کشاورزی ……………………….100

جدول 4-8- سختی نمونه‌های آب و پساب 103

جدول 4-9- درصد سدیم محلول نمونه‌های آب و پساب 104

جدول 4-10- غلظت برخی فلزات سنگین در نمونه‌های آب حوضه آبریز کارون…..107

جدول4-11-  غلظت برخی فلزات سنگین در نمونه‌های پساب ورودی به رودخانه. 109

جدول 4-12- خلاصه آماری نمونه‌های آب حوضه آبریز کارون 111

جدول4-13- خلاصه آماری نمونه‌های پساب ورودی به آّب حوضه آبریز کارون 111

جدول4-14- مقایسه میانگین غلظت عناصر آب حوضه آبریز کارون با برخی     

                    دیگر از رودخانه­های جهان ……………………………………….. 134

        جدول 4-15- آزمون نرمال بودن توزیع عناصر و یون های اصلی

                          و پارامترهای فیزیکوشیمیایی آب رودخانه …………………………. 147

        جدول 4-16- تحلیل عاملی فلزات سنگین نمونه‌های آب …………………………..152

        جدول 4-17- نتایج حاصل از مقایسه میانگین غلظت عناصر در آب

                         پساب (t- test)………………………………………………………………….154

 

فهرست اشکال

 

عنوان                                                                                                                     صفحه

شکل2-1- نقشه جغرافیایی محدوده مطالعاتی.. 25

شکل2-2- حوضه آبریز کارون.. 37

شکل2-3نقشه زمین شناسی منطقه مورد مطالعه. 39

شکل3-1- موقعیت نقاط نمونه برداری از آب رودخانه 53

شکل3-2- موقعیت نقاط نمونه برداری از پساب ورودی به رودخانه. 54

شکل3-3-  نمونه­برداری از آب رودخانه. 58

        شکل 3-4- نمونه­برداری از پساب……………………………………………………..58

        شکل 3-5- اندازه­گیری پارامتر­های آب………………………………………………………..59

        شکل 3-6- آماده سازی نمونه های آب ………………………………………………59

        شکل 3-7 تجزیه به روش ICP-MS ………………………………………………….61

شکل4-1- هدایت الکتریکی نمونه های آب رودخانه در ایستگاههای مختلف… 80

شکل4-2-  غلظت کلسیم در ایستگاههای مختلف… 83

شکل4-3- نمودار هیستوگرام کلسیم …………………………………………………83

شکل4-4- تغییرات منیزیم در ایستگاههای مختلف 84

شکل4-5- نمودار هیستوگرام منیزیم 85

شکل4-6- تغییرات غلظت پتاسیم در ایستگاههای مختلف 86

شکل4-7-نمودار هیستوگرام پتاسیم.. 86

شکل4-8- تغییرات غلظت سدیم در ایستگاههای مختلف 87

شکل4-9- نمودار هیستوگرام سدیم 87

شکل4-10- تغییرات غلظت کلر در ایستگاه های مختلف… 89

شکل4-11- نمودار هیستوگرام کلر 89

عنوان                                                                                                      صفحه

شکل4-12- تغییرات غلظت سولفات در ایستگاههای مختلف 90

شکل4-13- نمودار هیستوگرام سولفات 91

شکل4-14- تغییرات غلظت بیکربنات در ایستگاههای مختلف 92

شکل4-15- نمودار هیستوگرام بیکربنات 92

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شکل 4-35- نمودار هیستوگرام مولیبدن ………………………………………….123

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شکل 4- 38- نمودار تغییرات غلظت سرب در ایستگاه‌های مختلف ……………………….126

شکل 4-39- نمودار هیستوگرام سرب ……………………………………………………..126

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شکل 4-41- نمودار تغییرات غلظت سلنیم در ایستگاه‌های مختلف………………………..128

شکل 4-42- نمودارهیستوگرام سلنیم  ……………………………………………………128

شکل 4-43- نمودار تغییرات روی در ایستگاههای مختلف …………………………………130

شکل 4-44- نمودار هیستوگرام روی ………………………………………………………130

شکل 4-45- نمودار تغییرات وانادیم در ایستگاههای مختلف……………………………….131

شکل 4-46- نمودار هیستوگرام وانادیم  ……………………………………………………131

شکل 4-47- نمودار تغییرات جیوه در ایستگاههای مختلف ………………………………..132

شکل 4-48- نمودار هیستوگرام جیوه ……………………………………………………..132

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شکل 4-50- نمودار افزودگی-کاهیدگی نمونه های پساب ورودی به رودخانه………………141

شکل 4-51- نمودار تغییرات غلظت جیوه در نمونه های آب رودخانه و پساب …………….145

شکل 4-52- نتایج تحلیل خوشه­ای غلظت فلزات سنگین نمونه‌های آب  …………………149

شکل 4-53- نتایج تحلیل خوشه­ای غلظت یون­های اصلی نمونه‌های آب ………………….150

شکل 4- 54- نمودار Scree فلزات سنگین ………………………………………………..151

شکل 4-55- نقشه پراکنش فاکتور 1 آزمون تحلیل عاملی ………………………………..153

                  

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