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دانلود پروژه: تولید نانوکامپوزیت PE/SiO2به روش پلیمریزاسیون درجا

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تولید نانوکامپوزیت PE/SiO2به روش پلیمریزاسیون درجا

کارشناسی ارشد مهندسی شیمی- نانو

پلی اتیلن ها، بیشترین سهم تولید پلاستیک ها را در جهان به خود اختصاص داده اند. این پلیمرها در کنار کاربرد گسترده ی خود، دارای نقاط ضعفی در خواص مکانیکی هستند که این نقاط ضعف را می توان با تهیه کامپوزیت های مربوطه از طریق افزایش فیلرها و تقویت کننده هائی از قبیل سیلیکا(SiO2)، تالک، کربنات کلسیم و کربن بلک بهبود بخشید.

هدف از پروژه حاضر تولید آزمایشگاهی نانوکامپوزیت های پلی اتیلن – نانوسیلیکا با استفاده از پلیمریزاسیون درجا می‍باشد. به منظور انجام این پلیمریزاسیون، از سیستم کاتالیستی زیگلر-ناتا با دو پایه نانوسیلیکا و بوتیل اکتیل منیزیم(BOM) استفاده شد و در نهایت، کاتالیست تهیه شده جهت پلیمریزاسیون اتیلن مورد استفاده قرار گرفت. از بین ترکیبات معرفی شده بعنوانكاتاليستبرای کاتالیست های زیگلر-ناتا، بیشترین بازده مربوط بهTiCl4 است، لذا در پروژه حاضر،TiCl4بعنوان کاتالیست و تری اتیل آلومینیوم (TEAL) بعنوان کوکاتالیست یا فعال کننده انتخاب شده اند. از آنجایی که بازده سیستم کاتالیستی زیگلرناتا به شدت به حضور آب و هوا حساس است، کلیه مراحل ساخت کاتالیست و نانوکامپوزیت، تحت محیط گاز بی اثر نیتروژن انجام گرفت.

حضور نانوذرات سیلیکا درون زمینه پلیمر با آزمون های FT-IRتایید شد و همچنین TEMنشان دهنده ی توزیع مناسب و مؤثر نانوذرات سیلیکا در ماتریس پلی اتیلن می باشد. مورفولوژيپايه ،كاتاليستوپودرپليمريتهيهشدهبا تصاویر SEMوخواص حرارتی نانوکامپوزیت های تولیدی توسط آزمون های TGAو DSCبررسی شدند. نتایج این تست ها نشان دهنده یکاهش کریستالیتینه، عدم تغییر دمای ذوب و کریستالیزاسیون و هم چنین بهبود خوب پایداری حرارتی نمونه ها با افزایش مقدار کمی از نانوذرات سیلیکا می باشد.

کلمات کلیدی: پلیمریزاسیون درجا، پلی اتیلن، کاتالیست زیگلر-ناتا، نانوسیلیکا.

دسته: , برچسب: , , ,

1-1- سیلیس.. 13

1-2- فازهایسیلیس.. 14

1-3- نانوفناوری.. 16

1-4- نانوکامپوزیتها.. 16

1-4-1- انواعنانوکامپوزیتها.. 17

1-4-1-1- نانوکامپوزیتهایپایهسرامیکی.. 17

1-4-1-2- نانوکامپوزیتهایپایهفلزی.. 18

1-4-1-3- نانوکامپوزیتهایپایهپلیمری.. 18

1-4-2- نانوکامپوزیتهایباماتریسپلیمری.. 19

1-4-3- طبقهبندینانوکامپوزیتهایپلیمری.. 19

1-4-3-1- طبقهبندینانوکامپوزیتهایپلیمریبراساسابعاد.. 19

1-4-3-2- طبقهبندینانوکامپوزیتهایپلیمریبراساسنوعماتریسپلیمری   20

1-4-4- روشهایتولیدنانوکامپوزیتهایپلیمری.. 22

1-4-4-1- روشمحلولی.. 23

1-4-4-2- پلیمریزاسیوندرجا.. 24

1-4-4-3- روشمذاب.. 24

1-5- کاتالیستهایزیگلر-ناتا.. 25

1-5-1- نکاتمهمدرساختکاتالیستهایزیگلر-ناتا.. 28

1-5-2- کاتالیستهایزیگلر-ناتاازآغازتاامروز.. 29

1-5-3- نقشدانرداخلیدرکاتالیستهایزیگلر-ناتا.. 31

1-5-4- اجزاکاتالیستهایزیگلر-ناتا.. 32

1-5-4-1- کاتالیست.. 32

1-5-4-2- کوکاتالیست.. 32

1-5-4-3- پایه.. 33

1-5-6- نقشهیدروژندرپلیمریزاسیونکاتالیزورهایزیگلرناتا.. 34

1-6-تهيهنانوكامپوزيتهايپلياولفينيبهروشپليمريزاسيوندرجا   35

1-7-روشهایعملیسیستمهایپلیمریزاسیونزیگلر- ناتا.. 35

1-7-1- پلیمریزاسیونتودهای.. 35

1-7-2- پلمیریزاسیونمحلولی.. 36

1-7-3- پلیمریزاسیوندوغابی.. 36

1-7-4- پلیمریزاسیونگازی (راکتورهایبسترسیال).. 37

فصل دوم

2-1- بررسیکارهایمربوطبهتولیدنانوکامپوزیتهابافیلرنانوسیلیکا   39

2-2- بررسیکارهایمربوطبهتولیدنانوکامپوزیتهایباماتریسپلیاولفینباروشپلیمریزاسیوندرجا.. 46

فصل سوم

3-1- تجهیزاتودستگاهها.. 52

3-1-1- گلاوباکس.. 52

3-1-2- راكتورساختكاتاليست.. 53

3-1-3- سيستمپليمريزاسيون.. 54

3-1-3-1- راكتوربوچي.. 55

3-1-3-2- سيستمگرمايشوسرمايش.. 55

3-1-3-3- MFC.. 55

3-1-3-4- نمایشگر.. 56

3-1-3-5- كامپيوتر.. 56

3-1-4- هيترهمزنهايدولف.. 56

3-1-5- آون.. 56

3-1-6- دستگاهكارل-فيشر.. 56

3-2- موادمورداستفاده.. 57

3-2-1- گازنیتروژن.. 57

3-2-2- گازاتیلن.. 57

3-2-3- نانوسیلیکا.. 57

3-2-4- کاتالیست.. 57

3-2-5- کوکاتالیست.. 57

3-2-6- بوتیلاکتیلمنیزم.. 58

3-2-7- حلال.. 58

3-3- تستهایانجامشدهجهتتعیینخواصنانوکامپوزیتها.. 58

3-3-1- دستگاهکالریمترپویشیتفاضلی (DSC).. 58

3-3-2- دستگاهBET. 59

3-3-3- طیفسنجیFT-IR.. 60

3-3-4- دستگاهمیکروسکوپالکترونیروبشی (SEM).. 60

3-3-5- آزمونTGA.. 61

3-3-6- دستگاهTEM… 61

3-3-7- اندازهگیریبازدهکاتالیست.. 61

3-4- مراحلتولیدنانوکامپوزیتها.. 62

3-4-1- آمادهسازیپایهSilica- BOM… 62

3-4-2- ساختکاتالیست.. 62

3-4-3- پلیمریزاسیوناتیلن.. 63

3-4-3-1- آمادهسازیراکتور.. 63

3-4-3-2- تزریقحلالوکاتالیست.. 64

3-4-3-3- تزریقکاتالیستوآغازپلیمریزاسیون.. 64

3-5- تهیهنانوکامپوزیتاتیلن / سیلیکابامقادیرمختلفنانوذراتسیلیکا   65

3-6- خشککردنحلالها.. 65

فصل چهارم

4-1- آناليزپايه.. 67

4-1-1- اسپكتروسكوپيFT-IR.. 68

3-1-2- آنالیزBET. 72

4-2- آناليزكاتاليست.. 72

4-2-1- آنالیزعنصری.. 72

4-2-2- بررسيطيفهایFT-IR.. 72

4-2-3- آناليزBET. 73

4-3- اثرهيدروژنبرپليمريزاسيون.. 74

4-4- آناليزپليمرهايتوليدشده.. 75

4-4-1- آزمونDSC.. 75

4-4-2- تصویرTEM… 78

4-4-3- طیفFT-IR.. 79

4-4-4- آزمونTGA.. 81

4-4-5- آزمونSEM… 82

فصل پنجم

5-1- نتیجهگیری.. 87

5-2- پیشنهادات.. 89

فصل ششم

6-1- منابع.. 91

 

فهرست اشکال

شکل1-1-تهیهنانوکامپوزیتبهروشمحلولی.. 23

شکل 1-2– مراحلتهیهنانوکامپوزیتبهروشپلیمریزاسیوندرجا   24

شکل 1-3-مراحلروشمذاب.. 25

شکل 1-4-مهمترینترکیباتکاتالیستوکوکاتالیست.. 28

شکل 2-1– (aپلیپروپیلنخالص(bنانوکامپوزیتPP/SiO2 40

شکل 2-2-نمودارذوب(aپلیپروپیلنخالص(bنانوکامپوزیتPP/SiO2 41

شکل 2-3-نمودارکریستالینیته(aپلیپروپیلنخالص(bنانوکامپوزیتPP/SiO2 41

شکل 2-4-آنالیزFT-IRسیلیکااصلاحنشده.. 43

شکل 2-5-آنالیزFT-IRسیلیکااصلاحشده.. 43

شکل 2-6-تصاویرTEMنانوذراتSiO2تهیهشدهباروشسل-ژل(aNS20(b NS100. 45

شکل 2-7-تصاویرSEMa)پلیاتیلنتولیدیb )کاتالیستSiO2/MgCl2 (spherical)/TiCl4 47

شکل 2-8-نتایجتستکششکامپوزیتIPCدردرصدهایمختلفپالیگورسکیت   48

شکل 2-9-منحنیتغییراتکریستالینیتهکامپوزیتPE/Palygorskitبامیزانفیلر   48

شکل 3-1-شماييازگلاوباكس.. 53

شکل 3-2-شماييازسيستمپليمريزاسيون.. 54

شکل 4-1-شماتیکواکنشSilicaباBOM… 68

شکل 4-2-طیفFT-IRنمونهنانوذرهسیلیکاخالص.. 69

شکل 4-3-طیفFT-IRپایهSilica-BOM… 70

شکل 4-4-طیفFT-IRنانوذرهسیلیکاوپایهSilica-BOM… 71

شکل 4-5-طیفIRکاتالیست.. 73

شکل 4-6-ترموگرامDSCپليمرتوليدشده.. 75

شکل 4-7-تغییراتدرصدکریستالینیتینمونههابامیزاننانوذراتسیلیکا   77

شکل 4-8-تغییراتدمایذوبودمایکریستالیزاسیوننمونههابامیزاننانوذراتسیلیکا   77

شکل 4-9-تصاویرTEMنانوکامپوزیت.. 78

شکل 4-10-طیفFT-IRپلیاتیلن.. 79

شکل 4-11-طیفFT-IRپلیاتیلنتهیهشدهباکاتالیستبرپایهنانوسیلیکا   80

شکل 4-12-مقایسهطیفFT-IRپلیاتیلنوپلیمرتهیهشدهباکاتالیستبرپایهنانوسیلیکا   80

شکل 4-13-تصاویرSEMنانوسیلیکا.. 82

شکل 4-14-تصاویرSEMذراتSiO2-BOM… 83

شکل 4-15- تصاویرSEMگرفتهشدهازكاتاليست.. 84

شکل 4-16-تصویرSEMذراتپلیمرتولیدشده.. 85

 

 

 

فهرست جداول

جدول 1-1-انواعكاتاليستهايزيگلر-ناتا.. 32

جدول 1-2-انواعفعالكنندهها.. 33

جدول 1-3-انواعپایهها.. 34

جدول 2-1-قطروسطحویژهیسیلیکا.. 45

جدول 4-1-نتایجآزمونBET. 72

جدول 4-2-نتایجحاصلازآزمونBET. 73

جدول 4-3-اثرمقدارهيدروژنبربازدهكاتاليست.. 74

جدول 4-4-نتايجآزمونDSC.. 76

جدول 4-5- نتایجحاصلازآنالیزTGA.. 81

 

 

 

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اثر ترکیبات شیمیایی بازدارنده رشد جوانه های جانبی بر عملکرد کمی و کیفی توتون نر عقیم گرمخانه ای Nc100

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قیمت اصلی 37,000 تومان بود.قیمت فعلی 23,000 تومان است.
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قیمت اصلی 39,000 تومان بود.قیمت فعلی 21,000 تومان است.

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