فهرست مطالب
عنوان صفحه
چکیده 1
فصل اول : مقدمـــه
مقدمه. 3
1-1- بسته بندی.. 4
1-2- پلیمر سنتزی.. 4
1-3- پلیمر زیست تخریب پذیر. 5
1-3-1- پلی لاکتیک اسید (PLA) 5
1-4- فناوری نانو. 6
1-4-1- نانو. 6
1-5- کامپوزیت، نانوکامپوزیت، بایونانوکامپوزیت… 6
1-6- نقره 7
1-7- اهداف پژوهش… 7
1-8- فرضیات پژوهش… 8
فصل دوم : مروری بر تحقیقات انجام شده
2-1- بسته بندی.. 10
2-1-1- تعریف بسته بندی.. 11
2-1- 2- هدف از بسته بندی.. 11
2-1-3- خصوصیات مواد اولیه بسته بندی.. 12
2-2- بسته بندی فعال. 12
2-2-1- انواع سیستم های بسته بندی فعال. 13
2-2-1-1- بسته بندی جاذب اکسیژن. 13
2-1-2-2- بسته بندی متصاعد كننده دي اكسيد كربن.. 13
2-2-1-3- بسته بندی جاذب رطوبت.. 14
2-2-1-4- بسته بندی منتشركننده اتانول. 14
2-2-1-5- بسته بندی منتشركننده / جاذب طعم. 14
2-2-1-6- بسته بندی آنتی اکسیدانی.. 14
2-2-1-7- بسته بندی ضد ميكروبي.. 15
2-3- بسته بندی های ضد میکروبی.. 15
2-3-1- ویژگی های ترکیب ضد میکروب.. 16
2-4- فیلم و پوشش بسته بندی.. 17
2-4-1- کاربرد فیلم و پوشش های بسته بندی.. 17
2-4-2- ترکیب فیلم و پوشش های بسته بندی.. 17
2-5- پلیمرهای سنتزی.. 18
2-6- پلیمرهای زیست تخریب پذیر. 18
2-6-1- طبقه بندی پلیمرهای زیست تخریب پذیر. 20
2-6-2- مزایای پلیمرهای زیست تخریب پذیر. 21
2-6-3- پلی لاکتیک اسید. 22
2-6-3-1- خصوصیات پلی لاکتیک اسید. 23
2-6-3-2- محدودیت پلی لاکتیک اسید. 25
2-7- فناوری نانو. 25
2-7-1- نانو. 25
2-7-2- کاربرد فناوری نانو در صنعت بسته بندی مواد غذایی.. 26
2-8- کامپوزیت، نانو کامپوزیت و بایو نانو کامپوزیت… 27
2-9- نقره 28
2-9-1- مکانیسم عملکرد نقره در برابر باکتری.. 29
2-10- اشرشیا کلی.. 31
2-10-1- بیماریزایی اشرشیا کلی.. 31
2-10-2- عفونت های ناشی از اشرشیا کلی.. 32
2-11- تهیه و آماده سازی فیلم. 33
2-12- فرآیندهای ساخت فیلم. 34
2-13- مروری بر تحقیقات انجام شده 35
فصل سوم : مواد و روش ها
3-1- مواد شیمیایی.. 47
3-2- روش تهیه نانوکامپوزیت پلی لاکتیک اسید/ نقره 47
3-2-1- تهیه نانوکامپوزیت پلی لاکتیک اسید/ نقره با استفاده از کلوئید نانو نقره 48
3-2-2- تهیه نانوکامپوزیت پلی لاکتیک اسید/نقره با استفاده از پودر نانو نقره 49
3-3- آزمایشات… 50
3-3-1- بررسی فعالیت ضد میکروبی فیلم نانوکامپوزیت پلی لاکتیک اسید/نقره 50
3-3-1-1- باکتری مورد استفاده و روش فعالسازی آن. 50
3-3-1-2- بررسی فعالیت ضد میکروبی.. 50
3-3-2- طیف سنجی مادون قرمز با تبدیل فوریر ( FTIR) 52
3-3-3- آزﻣﻮن ﭘﺮاش ﭘﺮﺗﻮ اﻳﻜﺲ (XRD) 52
3-4-تجزیه و تحلیل آماری.. 54
فصل چهارم : نتایج و بحث
4-1- آنالیز فعالیت ضد میکروبی فیلم نانوکامپوزیت پلی لاکتیک اسید/نقره 56
4-2- طیف سنجی مادون قرمز ( FTIR) 60
4-3- آنالیز آزﻣﻮن ﭘﺮاش ﭘﺮﺗﻮ اﻳﻜﺲ (XRD) 61
4-3-1- آزﻣﻮن ﭘﺮاش ﭘﺮﺗﻮ اﻳﻜﺲ نانو ذرات نقره 61
4-3-2- آزﻣﻮن ﭘﺮاش ﭘﺮﺗﻮ اﻳﻜﺲ نانو ذرات دی اکسید تیتانیوم. 63
فصل پنجم : نتیجه گیری
5-1- بحث و نتیجه گیری.. 66
5-2- پیشنهادات… 68
منابع. 69
چکیده انگلیسی ……………………………………………………………………………………………………………… 80
فهرست جدول ها
عنوان جدول |
صفحه |
|
جدول (2-1): ویژگی های شیمیایی پلی لاکتیک اسید ………………………………………………………………. |
24 |
|
جدول (3-1): لیست مواد شیمیایی مورد استفاده در تهیه نانوکامپوزیت پلی لاکتیک اسید/ نقره …………. |
47 |
|
جدول (4-1): پارامترهای رشد میکروارگانیسم اشرشیاکلی در تماس با نانوکامپوزیت پلی لاکتیک اسید/ نقره بر طبق معادله گومپرتز …………………………………………………………………………………………… |
57 |
|
جدول (4-2): پارامترهای رشد میکروارگانیسم اشرشیاکلی در تماس با نانوکامپوزیت پلی لاکتیک اسید/ نقره بر طبق معادله لجستیک ………………………………………………………………………………………….. |
57 |
|
فهرست شکل ها
عنوان شکل |
صفحه |
|
شکل(2-1) : مکانیسم اثر نانو ذرات نقره بر سلول باکتری………………………………………………………. |
30 |
|
شکل( 3-1) : تهیه نانوکامپوزیت پلی لاکتیک اسید/نقره با استفاده از کلوئید نانو نقره ………………… |
48 |
|
شکل(3-2) : تهیه نانوکامپوزیت پلی لاکتیک اسید/ نقره با استفاده از پودر نانو نقره …………………… |
49 |
|
شکل (3-3) : بررسی تاثیر ضدمیکروبی بر پارامتر های رشد باکتر اشرشیاکلی با روش dynamic-Flask test ……………………………………………………………………………………………………………………… |
51 |
|
شکل (3-4) : دستگاه مادون قرمز با تبدیل فوریر………………………………………………………………….. |
52 |
|
شکل (3-5) : دستگاه ﭘﺮاش ﭘﺮﺗﻮ اﻳﻜﺲ (XRD) ………………………………………………………………… |
53 |
|
شکل (4-1) : منحنی رشد باکتری اشرشیا کلی …………………………………………………………………….. |
59 |
|
شکل (4-2) : طیف FTIR نانوکامپوزیت پلی لاکتیک اسید/نقره………………………………………………. |
60 |
|
شکل (4-3) : ﭘﺮاش ﭘﺮﺗﻮ اﻳﻜﺲ (XRD) نانوذرات نقره در فیلم پلی لاکتیک اسید و نانوکامپوزیت های پلی لاکتیک اسید/نقره ………………………………………………………………………………………………… |
62 |
|
شکل (4-4) : ﭘﺮاش ﭘﺮﺗﻮ اﻳﻜﺲ (XRD) نانوذرات دی اکسید تیتانیوم در فیلم پلی لاکتیک اسید و نانوکامپوزیت های پلی لاکتیک اسید/نقره …………………………………………………………………………….. |
64 |
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